Structures of six industrial benzimidazolone pigments from laboratory powder diffraction data

Publikation: Bidrag til tidsskrift › Tidsskriftartikel › Forskning › fagfællebedømt

Standard

Structures of six industrial benzimidazolone pigments from laboratory powder diffraction data. / van de Streek, Jacco; Brüning, Jürgen; Ivashevskaya, Svetlana N; Ermrich, Martin; Paulus, Erich F; Bolte, Michael; Schmidt, Martin.

I: Acta Crystallographica. Section B: Structural Science, Bind 65, Nr. Pt 2, 2009, s. 200-11.

Publikation: Bidrag til tidsskrift › Tidsskriftartikel › Forskning › fagfællebedømt

Harvard

van de Streek, J, Brüning, J, Ivashevskaya, SN, Ermrich, M, Paulus, EF, Bolte, M & Schmidt, M 2009, 'Structures of six industrial benzimidazolone pigments from laboratory powder diffraction data', Acta Crystallographica. Section B: Structural Science, bind 65, nr. Pt 2, s. 200-11. https://doi.org/10.1107/S0108768108041529

APA

van de Streek, J., Brüning, J., Ivashevskaya, S. N., Ermrich, M., Paulus, E. F., Bolte, M., & Schmidt, M. (2009). Structures of six industrial benzimidazolone pigments from laboratory powder diffraction data. Acta Crystallographica. Section B: Structural Science, 65(Pt 2), 200-11. https://doi.org/10.1107/S0108768108041529

Vancouver

van de Streek J, Brüning J, Ivashevskaya SN, Ermrich M, Paulus EF, Bolte M o.a. Structures of six industrial benzimidazolone pigments from laboratory powder diffraction data. Acta Crystallographica. Section B: Structural Science. 2009;65(Pt 2):200-11. https://doi.org/10.1107/S0108768108041529

Author

van de Streek, Jacco ; Brüning, Jürgen ; Ivashevskaya, Svetlana N ; Ermrich, Martin ; Paulus, Erich F ; Bolte, Michael ; Schmidt, Martin. / Structures of six industrial benzimidazolone pigments from laboratory powder diffraction data. I: Acta Crystallographica. Section B: Structural Science. 2009 ; Bind 65, Nr. Pt 2. s. 200-11.

Bibtex

@article{fbf1f7c341b3442ea69213b5fa5ea8c8,
title = "Structures of six industrial benzimidazolone pigments from laboratory powder diffraction data",
abstract = "The crystal structures of six industrially produced benzimidazolone pigments [Pigment Orange 36 (beta phase), Pigment Orange 62, Pigment Yellow 151, Pigment Yellow 154 (alpha phase), Pigment Yellow 181 (beta phase) and Pigment Yellow 194] were determined from laboratory X-ray powder diffraction data by means of real-space methods using the programs DASH and MRIA, respectively. Subsequent Rietveld refinements were carried out with TOPAS. The crystal phases correspond to those produced industrially. Additionally, the crystal structures of the non-commercial compound 'BIRZIL' (a chloro derivative of Pigment Yellow 194) and of a dimethylsulfoxide solvate of Pigment Yellow 154 were determined by single-crystal structure analyses. All eight crystal structures are different; the six industrial pigments even exhibit five different hydrogen-bond topologies. Apparently, the good application properties of the benzimidazolone pigments are not the result of one specific hydrogen-bonding pattern, but are the result of a combination of efficient molecular packing and strong intermolecular hydrogen bonds.",
author = "{van de Streek}, Jacco and J{\"u}rgen Br{\"u}ning and Ivashevskaya, {Svetlana N} and Martin Ermrich and Paulus, {Erich F} and Michael Bolte and Martin Schmidt",
year = "2009",
doi = "10.1107/S0108768108041529",
language = "English",
volume = "65",
pages = "200--11",
journal = "Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials",
issn = "2052-5192",
publisher = "Wiley",
number = "Pt 2",

}

RIS

TY - JOUR

T1 - Structures of six industrial benzimidazolone pigments from laboratory powder diffraction data

AU - van de Streek, Jacco

AU - Brüning, Jürgen

AU - Ivashevskaya, Svetlana N

AU - Ermrich, Martin

AU - Paulus, Erich F

AU - Bolte, Michael

AU - Schmidt, Martin

PY - 2009

Y1 - 2009

N2 - The crystal structures of six industrially produced benzimidazolone pigments [Pigment Orange 36 (beta phase), Pigment Orange 62, Pigment Yellow 151, Pigment Yellow 154 (alpha phase), Pigment Yellow 181 (beta phase) and Pigment Yellow 194] were determined from laboratory X-ray powder diffraction data by means of real-space methods using the programs DASH and MRIA, respectively. Subsequent Rietveld refinements were carried out with TOPAS. The crystal phases correspond to those produced industrially. Additionally, the crystal structures of the non-commercial compound 'BIRZIL' (a chloro derivative of Pigment Yellow 194) and of a dimethylsulfoxide solvate of Pigment Yellow 154 were determined by single-crystal structure analyses. All eight crystal structures are different; the six industrial pigments even exhibit five different hydrogen-bond topologies. Apparently, the good application properties of the benzimidazolone pigments are not the result of one specific hydrogen-bonding pattern, but are the result of a combination of efficient molecular packing and strong intermolecular hydrogen bonds.

AB - The crystal structures of six industrially produced benzimidazolone pigments [Pigment Orange 36 (beta phase), Pigment Orange 62, Pigment Yellow 151, Pigment Yellow 154 (alpha phase), Pigment Yellow 181 (beta phase) and Pigment Yellow 194] were determined from laboratory X-ray powder diffraction data by means of real-space methods using the programs DASH and MRIA, respectively. Subsequent Rietveld refinements were carried out with TOPAS. The crystal phases correspond to those produced industrially. Additionally, the crystal structures of the non-commercial compound 'BIRZIL' (a chloro derivative of Pigment Yellow 194) and of a dimethylsulfoxide solvate of Pigment Yellow 154 were determined by single-crystal structure analyses. All eight crystal structures are different; the six industrial pigments even exhibit five different hydrogen-bond topologies. Apparently, the good application properties of the benzimidazolone pigments are not the result of one specific hydrogen-bonding pattern, but are the result of a combination of efficient molecular packing and strong intermolecular hydrogen bonds.

U2 - 10.1107/S0108768108041529

DO - 10.1107/S0108768108041529

M3 - Journal article

C2 - 19299876

VL - 65

SP - 200

EP - 211

JO - Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials

JF - Acta Crystallographica Section B: Structural Science, Crystal Engineering and Materials

SN - 2052-5192

IS - Pt 2

ER -

ID: 44254353